Crystallography Open Database

Information card for entry 4327480

Preview

Coordinates	4327480.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C134.5 H111 Ag2 Cl6.5 F3 O15.25 P4 S5
Calculated formula	C134.5 H111 Ag2 Cl6.5 F3 O15.25 P4 S5
Title of publication	Tetraphosphinitoresorcinarene Complexes: Dynamic Clusters with Silver(I) and Copper(I) Halides
Authors of publication	Dana J. Eisler; Christopher W. Kirby; Richard J. Puddephatt
Journal of publication	Inorganic Chemistry
Year of publication	2003
Journal volume	42
Pages of publication	7626 - 7634
a	18.426 ± 0.004 Å
b	19.698 ± 0.004 Å
c	21.242 ± 0.004 Å
α	79.25 ± 0.03°
β	73.09 ± 0.03°
γ	63.73 ± 0.03°
Cell volume	6600 ± 3 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	8
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1484
Residual factor for significantly intense reflections	0.0913
Weighted residual factors for significantly intense reflections	0.2436
Weighted residual factors for all reflections included in the refinement	0.2822
Goodness-of-fit parameter for all reflections included in the refinement	1.031
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4327480.cif
120105	2014-07-12	Adding DOIs to range 4/32 structures.	4327480.cif
61279	2012-06-26	cif/4 Fixing wrong year of publication of several entries (there was a mistake when these files were deposited)	4327480.cif
61251	2012-06-25	cif/ Adding structures of 4327480 via cif-deposit CGI script.	4327480.cif