Crystallography Open Database

Information card for entry 4330563

Preview

Coordinates	4330563.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C27 H27 Cl10 N6 Rh Sb
Calculated formula	C27 H27 Cl10 N6 Rh Sb
Title of publication	Syntheses and Electronic Properties of Rhodium(III) Complexes Bearing a Redox-Active Ligand
Authors of publication	Sarath Wanniarachchi; Brendan J. Liddle; Brandon Kizer; Jeewantha S. Hewage; Sergey V. Lindeman; James R. Gardinier
Journal of publication	Inorganic Chemistry
Year of publication	2012
Journal volume	51
Pages of publication	10572 - 10580
a	16.2675 ± 0.0004 Å
b	15.4317 ± 0.0003 Å
c	15.276 ± 0.0004 Å
α	90°
β	105.369 ± 0.003°
γ	90°
Cell volume	3697.68 ± 0.16 Å³
Cell temperature	100.2 ± 0.2 K
Ambient diffraction temperature	100.2 ± 0.2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0452
Residual factor for significantly intense reflections	0.0379
Weighted residual factors for significantly intense reflections	0.0935
Weighted residual factors for all reflections included in the refinement	0.0985
Goodness-of-fit parameter for all reflections included in the refinement	1.036
Diffraction radiation wavelength	1.5418 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179408 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/05.	4330563.cif
80016	2013-04-06	cif/ Adding structures of 4330563 via cif-deposit CGI script.	4330563.cif