Crystallography Open Database

Information card for entry 4330564

Preview

Coordinates	4330564.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C26.18 H33.35 Cl2.35 N5 P Rh
Calculated formula	C26.176 H33.352 Cl2.352 N5 P Rh
Title of publication	Syntheses and Electronic Properties of Rhodium(III) Complexes Bearing a Redox-Active Ligand
Authors of publication	Sarath Wanniarachchi; Brendan J. Liddle; Brandon Kizer; Jeewantha S. Hewage; Sergey V. Lindeman; James R. Gardinier
Journal of publication	Inorganic Chemistry
Year of publication	2012
Journal volume	51
Pages of publication	10572 - 10580
a	31.8629 ± 0.0006 Å
b	31.8629 ± 0.0006 Å
c	10.9579 ± 0.0003 Å
α	90°
β	90°
γ	90°
Cell volume	11124.9 ± 0.4 Å³
Cell temperature	102.1 K
Ambient diffraction temperature	102.1 K
Number of distinct elements	6
Space group number	88
Hermann-Mauguin space group symbol	I 41/a
Hall space group symbol	-I 4ad
Residual factor for all reflections	0.0566
Residual factor for significantly intense reflections	0.034
Weighted residual factors for significantly intense reflections	0.0612
Weighted residual factors for all reflections included in the refinement	0.0716
Goodness-of-fit parameter for all reflections included in the refinement	1.042
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179408 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/05.	4330564.cif
80017	2013-04-06	cif/ Adding structures of 4330564 via cif-deposit CGI script.	4330564.cif