Crystallography Open Database

Information card for entry 4330890

Preview

Coordinates	4330890.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C21 H35 N2 Rh Si2
Calculated formula	C21 H35 N2 Rh Si2
SMILES	[Rh]1234(N([Si](C)(C)C)C(=[N]1[Si](C)(C)C)c1ccccc1)[CH]1=[CH]2CC[CH]3=[CH]4CC1
Title of publication	Bis(amidinato)germylenerhodium Complexes: Synthesis, Structure, and Density Functional Theory Calculations
Authors of publication	Dimitri Matioszek; Nathalie Saffon; Jean-Marc Sotiropoulos; Karinne Miqueu; Annie Castel; Jean Escudié
Journal of publication	Inorganic Chemistry
Year of publication	2012
Journal volume	51
Pages of publication	11716 - 11721
a	6.6791 ± 0.0002 Å
b	9.7861 ± 0.0004 Å
c	34.6517 ± 0.0013 Å
α	90°
β	94.379 ± 0.002°
γ	90°
Cell volume	2258.3 ± 0.14 Å³
Cell temperature	193 ± 2 K
Ambient diffraction temperature	193 ± 2 K
Number of distinct elements	5
Space group number	7
Hermann-Mauguin space group symbol	P 1 n 1
Hall space group symbol	P -2yac
Residual factor for all reflections	0.0491
Residual factor for significantly intense reflections	0.0382
Weighted residual factors for significantly intense reflections	0.0681
Weighted residual factors for all reflections included in the refinement	0.0715
Goodness-of-fit parameter for all reflections included in the refinement	1.024
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179411 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/08.	4330890.cif
80349	2013-04-07	cif/ Adding structures of 4330890 via cif-deposit CGI script.	4330890.cif