Crystallography Open Database

Information card for entry 4330891

Preview

Coordinates	4330891.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C23 H35 N2 Rh
Calculated formula	C23 H35 N2 Rh
SMILES	C1(c2ccccc2)=[N](C(C)(C)C)[Rh]234([CH]5CC[CH]4=[CH]3CC[CH]2=5)N1C(C)(C)C
Title of publication	Bis(amidinato)germylenerhodium Complexes: Synthesis, Structure, and Density Functional Theory Calculations
Authors of publication	Dimitri Matioszek; Nathalie Saffon; Jean-Marc Sotiropoulos; Karinne Miqueu; Annie Castel; Jean Escudié
Journal of publication	Inorganic Chemistry
Year of publication	2012
Journal volume	51
Pages of publication	11716 - 11721
a	6.8114 ± 0.0006 Å
b	13.768 ± 0.0013 Å
c	11.0049 ± 0.0009 Å
α	90°
β	92.509 ± 0.003°
γ	90°
Cell volume	1031.04 ± 0.16 Å³
Cell temperature	193 ± 2 K
Ambient diffraction temperature	193 ± 2 K
Number of distinct elements	4
Space group number	11
Hermann-Mauguin space group symbol	P 1 21/m 1
Hall space group symbol	-P 2yb
Residual factor for all reflections	0.0319
Residual factor for significantly intense reflections	0.0273
Weighted residual factors for significantly intense reflections	0.0679
Weighted residual factors for all reflections included in the refinement	0.0709
Goodness-of-fit parameter for all reflections included in the refinement	1.056
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179411 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/08.	4330891.cif
80350	2013-04-07	cif/ Adding structures of 4330891 via cif-deposit CGI script.	4330891.cif