Crystallography Open Database

Information card for entry 4331130

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Structure parameters

Formula	C55.75 H43.5 Cl1.5 F10 I N P2 Pd Pt
Calculated formula	C55.75 H43.5 Cl1.5 F10 I N P2 Pd Pt
Title of publication	Formation of P-C Bond through Reductive Coupling between Bridging Phosphido and Benzoquinolinate Groups. Isolation of Complexes of the Pt(II)/Pt(IV)/Pt(II) Sequence
Authors of publication	Andersson Arias; Juan Forniés; Consuelo Fortuño; Antonio Martín; Mario Latronico; Piero Mastrorilli; Stefano Todisco; Vito Gallo
Journal of publication	Inorganic Chemistry
Year of publication	2012
Journal volume	51
Pages of publication	12682 - 12696
a	17.2984 ± 0.0003 Å
b	13.6095 ± 0.0002 Å
c	22.9239 ± 0.0004 Å
α	90°
β	96.7838 ± 0.0014°
γ	90°
Cell volume	5359.02 ± 0.15 Å³
Cell temperature	373 ± 2 K
Ambient diffraction temperature	373 ± 2 K
Number of distinct elements	9
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0683
Residual factor for significantly intense reflections	0.0349
Weighted residual factors for significantly intense reflections	0.059
Weighted residual factors for all reflections included in the refinement	0.0621
Goodness-of-fit parameter for all reflections included in the refinement	1.018
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
301839 (current)	2025-08-21	Add cross-references to PubChem compounds in COD range 4/33/ Each referenced PubChem compound corresponds to the full crystal structure.	4331130.cif
176467	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4331130.cif
80593	2013-04-08	cif/ Adding structures of 4331130 via cif-deposit CGI script.	4331130.cif