Crystallography Open Database

Information card for entry 4331131

Preview

Coordinates	4331131.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C53.5 H38.5 F10 I N P2 Pd2
Calculated formula	C53.5 H38.5 F10 I N P2 Pd2
Title of publication	Formation of P-C Bond through Reductive Coupling between Bridging Phosphido and Benzoquinolinate Groups. Isolation of Complexes of the Pt(II)/Pt(IV)/Pt(II) Sequence
Authors of publication	Andersson Arias; Juan Forniés; Consuelo Fortuño; Antonio Martín; Mario Latronico; Piero Mastrorilli; Stefano Todisco; Vito Gallo
Journal of publication	Inorganic Chemistry
Year of publication	2012
Journal volume	51
Pages of publication	12682 - 12696
a	17.1149 ± 0.0007 Å
b	13.7727 ± 0.0004 Å
c	22.9446 ± 0.0007 Å
α	90°
β	97.294 ± 0.003°
γ	90°
Cell volume	5364.7 ± 0.3 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.1095
Residual factor for significantly intense reflections	0.0795
Weighted residual factors for significantly intense reflections	0.2136
Weighted residual factors for all reflections included in the refinement	0.2254
Goodness-of-fit parameter for all reflections included in the refinement	1.068
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4331131.cif
80594	2013-04-08	cif/ Adding structures of 4331131 via cif-deposit CGI script.	4331131.cif