Crystallography Open Database

Information card for entry 4331487

Preview

Coordinates	4331487.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	K2PbGe2S6
Formula	Ge2 K2 Pb S6
Calculated formula	Ge2 K2 Pb S6
Title of publication	Exploratory Synthesis in Molten Salts: Role of Flux Basicity in the Stabilization of the Complex Thiogermanates Cs4Pb4Ge5S16, K2PbGe2S6, and K4Sn3Ge3S14
Authors of publication	Palchik, Oleg; Marking, Gregory M.; Kanatzidis, Mercouri G.
Journal of publication	Inorganic Chemistry
Year of publication	2005
Journal volume	44
Journal issue	12
Pages of publication	4151 - 4153
a	9.268 ± 0.002 Å
b	14.338 ± 0.003 Å
c	8.919 ± 0.002 Å
α	90°
β	90.563 ± 0.004°
γ	90°
Cell volume	1185.1 ± 0.4 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	4
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.021
Residual factor for significantly intense reflections	0.0181
Weighted residual factors for significantly intense reflections	0.0397
Weighted residual factors for all reflections included in the refinement	0.0405
Goodness-of-fit parameter for all reflections included in the refinement	1.057
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179417 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/14.	4331487.cif
97648	2014-01-29	cif/ Adding structures of 4331487 via cif-deposit CGI script.	4331487.cif