Crystallography Open Database

Information card for entry 4331488

Preview

Coordinates	4331488.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	Ge3 K4 S14 Sn3
Calculated formula	Ge3 K4 S14 Sn3
Title of publication	Exploratory Synthesis in Molten Salts: Role of Flux Basicity in the Stabilization of the Complex Thiogermanates Cs4Pb4Ge5S16, K2PbGe2S6, and K4Sn3Ge3S14
Authors of publication	Palchik, Oleg; Marking, Gregory M.; Kanatzidis, Mercouri G.
Journal of publication	Inorganic Chemistry
Year of publication	2005
Journal volume	44
Journal issue	12
Pages of publication	4151 - 4153
a	6.9442 ± 0.0016 Å
b	15.118 ± 0.004 Å
c	12.071 ± 0.003 Å
α	90°
β	100.508 ± 0.004°
γ	90°
Cell volume	1246 ± 0.5 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	4
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0413
Residual factor for significantly intense reflections	0.0246
Weighted residual factors for significantly intense reflections	0.0548
Weighted residual factors for all reflections included in the refinement	0.0589
Goodness-of-fit parameter for all reflections included in the refinement	1.106
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179417 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/14.	4331488.cif
97649	2014-01-29	cif/ Adding structures of 4331488 via cif-deposit CGI script.	4331488.cif