Crystallography Open Database

Information card for entry 4332732

Preview

Coordinates	4332732.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C30 H48 Cu4 K3 N6 O50 Si W11
Calculated formula	C30 H24 Cu4 K3 N6 O50 Si W11
Title of publication	Hybrid Inorganic−Metalorganic Compounds Containing Copper(II)-Monosubstituted Keggin Polyanions and Polymeric Copper(I) Complexes.
Authors of publication	San Felices, Leire; Vitoria, Pablo; Gutiérrez-Zorrilla, Juan M.; Lezama, Luis; Reinoso, Santiago
Journal of publication	Inorganic Chemistry
Year of publication	2006
Journal volume	45
Journal issue	19
Pages of publication	7748 - 7757
a	10.9722 ± 0.0004 Å
b	21.5961 ± 0.0007 Å
c	28.0216 ± 0.0008 Å
α	90°
β	90°
γ	90°
Cell volume	6639.9 ± 0.4 Å³
Cell temperature	295 ± 2 K
Ambient diffraction temperature	295 ± 2 K
Number of distinct elements	8
Space group number	54
Hermann-Mauguin space group symbol	P b c b
Hall space group symbol	-P 2bc 2b
Residual factor for all reflections	0.098
Residual factor for significantly intense reflections	0.0778
Weighted residual factors for significantly intense reflections	0.1477
Weighted residual factors for all reflections included in the refinement	0.1523
Goodness-of-fit parameter for all reflections included in the refinement	1.31
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179430 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/27.	4332732.cif
98512	2014-01-30	cif/ Adding structures of 4332732, 4332733, 4332734 via cif-deposit CGI script.	4332732.cif