Crystallography Open Database

Information card for entry 4332733

Preview

Coordinates	4332733.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C30 H47 Cu K N5 O45 Si W11
Calculated formula	C30 H35 Cu K N5 O45 Si W11
Title of publication	Hybrid Inorganic−Metalorganic Compounds Containing Copper(II)-Monosubstituted Keggin Polyanions and Polymeric Copper(I) Complexes.
Authors of publication	San Felices, Leire; Vitoria, Pablo; Gutiérrez-Zorrilla, Juan M.; Lezama, Luis; Reinoso, Santiago
Journal of publication	Inorganic Chemistry
Year of publication	2006
Journal volume	45
Journal issue	19
Pages of publication	7748 - 7757
a	10.8974 ± 0.0007 Å
b	13.1029 ± 0.001 Å
c	21.4442 ± 0.0013 Å
α	87.227 ± 0.006°
β	85.004 ± 0.005°
γ	84.328 ± 0.006°
Cell volume	3033 ± 0.4 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	8
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0984
Residual factor for significantly intense reflections	0.0448
Weighted residual factors for significantly intense reflections	0.0748
Weighted residual factors for all reflections included in the refinement	0.0822
Goodness-of-fit parameter for all reflections included in the refinement	0.813
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179430 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/27.	4332733.cif
98512	2014-01-30	cif/ Adding structures of 4332732, 4332733, 4332734 via cif-deposit CGI script.	4332733.cif