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Information card for entry 4333729
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| Coordinates | 4333729.cif |
|---|---|
| Structure factors | 4333729.hkl |
| Original paper (by DOI) | HTML |
| Formula | C30 H46 F2 N4 Sn2 |
|---|---|
| Calculated formula | C30 H46 F2 N4 Sn2 |
| Title of publication | Oxidative Addition Versus Substitution Reactions of Group 14 Dialkylamino Metalylenes with Pentafluoropyridine |
| Authors of publication | Prinson P. Samuel; Amit Pratap Singh; Sankaranarayana Pillai Sarish; Julia Matussek; Ina Objartel; Herbert W. Roesky; Dietmar Stalke |
| Journal of publication | Inorganic Chemistry |
| Year of publication | 2013 |
| Journal volume | 52 |
| Pages of publication | 1544 - 1549 |
| a | 10.149 ± 0.003 Å |
| b | 9.614 ± 0.002 Å |
| c | 16.921 ± 0.002 Å |
| α | 90° |
| β | 99.62 ± 0.02° |
| γ | 90° |
| Cell volume | 1627.8 ± 0.6 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/c 1 |
| Hall space group symbol | -P 2ybc |
| Residual factor for all reflections | 0.0205 |
| Residual factor for significantly intense reflections | 0.018 |
| Weighted residual factors for significantly intense reflections | 0.0409 |
| Weighted residual factors for all reflections included in the refinement | 0.0422 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.087 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | Yes |
| Revision | Date | Message | Files |
|---|---|---|---|
| 181932 (current) | 2016-04-07 | hkl/4/ (antanas@echidna.ibt.lt) Adding svn headers to multiple entries in subrange 4/33. |
4333729.cif 4333729.hkl |
| 180700 | 2016-04-02 | cod/ (antanas@echidna.ibt.lt) Setting the 'svn:keywords' property for all '*.hkl' files that were previously unaffected by this property. |
4333729.cif 4333729.hkl |
| 179440 | 2016-03-23 | cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/37. |
4333729.cif 4333729.hkl |
| 103164 | 2014-02-25 | hkl/4 Adding Fobs files for entries coming from J. Org. Chem. and Inorg. Chem. 2013 |
4333729.cif 4333729.hkl |
| 99533 | 2014-01-31 | cif/ Adding structures of 4333729 via cif-deposit CGI script. |
4333729.cif |
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Users of the data should acknowledge the original authors of the
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