Crystallography Open Database

Information card for entry 4335086

Preview

Coordinates	4335086.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C52 H104 Ag4 F24 N16 O16 P8 S4 Sb4
Calculated formula	C52 H104 Ag4 F24 N16 O16 P8 S4 Sb4
Title of publication	New Ag(I)-Iminophosphorane Coordination Polymers as Efficient Catalysts Precursors for the MW-Assisted Meyer-Schuster Rearrangement of Propargylic Alcohols in Water
Authors of publication	Joaquín García-Álvarez; Josefina Díez; Cristian Vidal; Cristian Vicent
Journal of publication	Inorganic Chemistry
Year of publication	2013
Journal volume	52
Pages of publication	6533 - 6542
a	13.3063 ± 0.0005 Å
b	14.7998 ± 0.0005 Å
c	25.4223 ± 0.0008 Å
α	92.271 ± 0.003°
β	91.468 ± 0.003°
γ	93.049 ± 0.003°
Cell volume	4993.5 ± 0.3 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	9
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1104
Residual factor for significantly intense reflections	0.0705
Weighted residual factors for significantly intense reflections	0.1775
Weighted residual factors for all reflections included in the refinement	0.2031
Goodness-of-fit parameter for all reflections included in the refinement	1.018
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179453 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/50.	4335086.cif
100990	2014-02-10	cif/ Adding structures of 4335086 via cif-deposit CGI script.	4335086.cif