Crystallography Open Database

Information card for entry 4335087

Preview

Coordinates	4335087.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C18 H22 Ag F6 N4 O2 P2 S Sb
Calculated formula	C18 H22 Ag F6 N4 O2 P2 S Sb
Title of publication	New Ag(I)-Iminophosphorane Coordination Polymers as Efficient Catalysts Precursors for the MW-Assisted Meyer-Schuster Rearrangement of Propargylic Alcohols in Water
Authors of publication	Joaquín García-Álvarez; Josefina Díez; Cristian Vidal; Cristian Vicent
Journal of publication	Inorganic Chemistry
Year of publication	2013
Journal volume	52
Pages of publication	6533 - 6542
a	10.6584 ± 0.0003 Å
b	10.8702 ± 0.0002 Å
c	10.9832 ± 0.0003 Å
α	84.351 ± 0.002°
β	88.716 ± 0.001°
γ	76.482 ± 0.001°
Cell volume	1231.24 ± 0.05 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	9
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0421
Residual factor for significantly intense reflections	0.03
Weighted residual factors for significantly intense reflections	0.0918
Weighted residual factors for all reflections included in the refinement	0.1272
Goodness-of-fit parameter for all reflections included in the refinement	1.149
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179453 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/50.	4335087.cif
100991	2014-02-10	cif/ Adding structures of 4335087 via cif-deposit CGI script.	4335087.cif