Crystallography Open Database

Information card for entry 4339224

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Structure parameters

Formula	C22 H14 N4 O5 Pb
Calculated formula	C22 H14 N4 O5 Pb
Title of publication	Organic-acid effect on the structures of a series of lead(II) complexes.
Authors of publication	Yang, Jin; Ma, Jian-Fang; Liu, Ying-Ying; Ma, Ji-Cheng; Batten, Stuart R.
Journal of publication	Inorganic chemistry
Year of publication	2007
Journal volume	46
Journal issue	16
Pages of publication	6542 - 6555
a	6.8124 ± 0.0014 Å
b	8.1738 ± 0.0016 Å
c	18.07 ± 0.004 Å
α	90.88 ± 0.03°
β	93.82 ± 0.03°
γ	102.61 ± 0.03°
Cell volume	979.3 ± 0.4 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.048
Residual factor for significantly intense reflections	0.0371
Weighted residual factors for significantly intense reflections	0.0768
Weighted residual factors for all reflections included in the refinement	0.08
Goodness-of-fit parameter for all reflections included in the refinement	1.077
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
301839 (current)	2025-08-21	Add cross-references to PubChem compounds in COD range 4/33/ Each referenced PubChem compound corresponds to the full crystal structure.	4339224.cif
176432	2016-02-14	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries.	4339224.cif
117216	2014-06-14	cif/ Adding structures of 4339221, 4339222, 4339223, 4339224, 4339225, 4339226, 4339227, 4339228, 4339229, 4339230 via cif-deposit CGI script.	4339224.cif