Crystallography Open Database

Information card for entry 4339225

Preview

Coordinates	4339225.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C86 H52 N18 O13 Pb2
Calculated formula	C86 H52 N18 O13 Pb2
Title of publication	Organic-acid effect on the structures of a series of lead(II) complexes.
Authors of publication	Yang, Jin; Ma, Jian-Fang; Liu, Ying-Ying; Ma, Ji-Cheng; Batten, Stuart R.
Journal of publication	Inorganic chemistry
Year of publication	2007
Journal volume	46
Journal issue	16
Pages of publication	6542 - 6555
a	22.067 ± 0.003 Å
b	18.186 ± 0.002 Å
c	19.244 ± 0.003 Å
α	90°
β	90°
γ	90°
Cell volume	7722.8 ± 1.8 Å³
Cell temperature	200 ± 2 K
Ambient diffraction temperature	200 ± 2 K
Number of distinct elements	5
Space group number	56
Hermann-Mauguin space group symbol	P c c n
Hall space group symbol	-P 2ab 2ac
Residual factor for all reflections	0.1222
Residual factor for significantly intense reflections	0.0725
Weighted residual factors for significantly intense reflections	0.1585
Weighted residual factors for all reflections included in the refinement	0.1814
Goodness-of-fit parameter for all reflections included in the refinement	1.177
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179495 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/92.	4339225.cif
117216	2014-06-14	cif/ Adding structures of 4339221, 4339222, 4339223, 4339224, 4339225, 4339226, 4339227, 4339228, 4339229, 4339230 via cif-deposit CGI script.	4339225.cif