Crystallography Open Database

Information card for entry 4339226

Preview

Coordinates	4339226.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C52 H30 N8 O9 Pb2
Calculated formula	C52 H28 N8 O9 Pb2
Title of publication	Organic-acid effect on the structures of a series of lead(II) complexes.
Authors of publication	Yang, Jin; Ma, Jian-Fang; Liu, Ying-Ying; Ma, Ji-Cheng; Batten, Stuart R.
Journal of publication	Inorganic chemistry
Year of publication	2007
Journal volume	46
Journal issue	16
Pages of publication	6542 - 6555
a	9.677 ± 0.003 Å
b	11.884 ± 0.004 Å
c	11.988 ± 0.004 Å
α	100.375 ± 0.005°
β	112.273 ± 0.004°
γ	95.158 ± 0.005°
Cell volume	1235.8 ± 0.7 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0581
Residual factor for significantly intense reflections	0.0519
Weighted residual factors for significantly intense reflections	0.1254
Weighted residual factors for all reflections included in the refinement	0.1296
Goodness-of-fit parameter for all reflections included in the refinement	1.012
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176432 (current)	2016-02-14	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries.	4339226.cif
117216	2014-06-14	cif/ Adding structures of 4339221, 4339222, 4339223, 4339224, 4339225, 4339226, 4339227, 4339228, 4339229, 4339230 via cif-deposit CGI script.	4339226.cif