Crystallography Open Database

Information card for entry 4343607

Preview

Coordinates	4343607.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H34 Si4
Calculated formula	C24 H34 Si4
SMILES	[SiH]([Si](c1ccccc1)(c1ccccc1)c1ccccc1)([Si](C)(C)C)[Si](C)(C)C
Title of publication	{Ge9[Si(SiMe3)2(SiPh3)]3}(-): Ligand Modification in Metalloid Germanium Cluster Chemistry.
Authors of publication	Kysliak, Oleksandr; Schrenk, Claudio; Schnepf, Andreas
Journal of publication	Inorganic chemistry
Year of publication	2015
Journal volume	54
Journal issue	14
Pages of publication	7083 - 7088
a	16.7748 ± 0.0019 Å
b	9.3516 ± 0.0011 Å
c	16.7511 ± 0.0018 Å
α	90°
β	90°
γ	90°
Cell volume	2627.8 ± 0.5 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	3
Space group number	33
Hermann-Mauguin space group symbol	P n a 21
Hall space group symbol	P 2c -2n
Residual factor for all reflections	0.0905
Residual factor for significantly intense reflections	0.0504
Weighted residual factors for significantly intense reflections	0.0912
Weighted residual factors for all reflections included in the refinement	0.1061
Goodness-of-fit parameter for all reflections included in the refinement	1.051
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176428 (current)	2016-02-13	Replaced deprecated COD CIF data names with their more modern alternatives. The _cod_cif_authors_sg_Hall and _cod_cif_authors_sg_H-M data items were renamed to _cod_original_sg_symbol_Hall and _cod_cif_authors_sg_H-M respectively.	4343607.cif
152834	2015-08-05	cif/ Updating files of 4343607, 4343608 Original log message: Adding full bibliography for 4343607--4343608.cif.	4343607.cif
141429	2015-07-09	cif/ Adding structures of 4343607 via cif-deposit CGI script.	4343607.cif