Crystallography Open Database

Information card for entry 4343608

Preview

Coordinates	4343608.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C220 H350 Ge18 Hg O19 Si24
Calculated formula	C220 H350 Ge18 Hg O19 Si24
Title of publication	{Ge9[Si(SiMe3)2(SiPh3)]3}(-): Ligand Modification in Metalloid Germanium Cluster Chemistry.
Authors of publication	Kysliak, Oleksandr; Schrenk, Claudio; Schnepf, Andreas
Journal of publication	Inorganic chemistry
Year of publication	2015
Journal volume	54
Journal issue	14
Pages of publication	7083 - 7088
a	19.1052 ± 0.0019 Å
b	20.27 ± 0.002 Å
c	20.835 ± 0.002 Å
α	112.591 ± 0.002°
β	108.382 ± 0.002°
γ	103.66 ± 0.002°
Cell volume	6454.9 ± 1.1 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0965
Residual factor for significantly intense reflections	0.0493
Weighted residual factors for significantly intense reflections	0.117
Weighted residual factors for all reflections included in the refinement	0.1394
Goodness-of-fit parameter for all reflections included in the refinement	1.03
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
176428 (current)	2016-02-13	Replaced deprecated COD CIF data names with their more modern alternatives. The _cod_cif_authors_sg_Hall and _cod_cif_authors_sg_H-M data items were renamed to _cod_original_sg_symbol_Hall and _cod_cif_authors_sg_H-M respectively.	4343608.cif
152834	2015-08-05	cif/ Updating files of 4343607, 4343608 Original log message: Adding full bibliography for 4343607--4343608.cif.	4343608.cif
141430	2015-07-09	cif/ Adding structures of 4343608 via cif-deposit CGI script.	4343608.cif