Crystallography Open Database

Information card for entry 4344047

Preview

Coordinates	4344047.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	(Ge9Si(SiMe3)3)Cu(Ge9Si(SiMe3)3)CuPPh3 2.5hex
Formula	C29 H70.67 Cu0.67 Ge6 P0.33 Si8
Calculated formula	C29 H70.6667 Cu0.666667 Ge6 P0.333333 Si8
Title of publication	Coordination of Tri-Substituted Nona-Germanium Clusters to Cu(I) and Pd(0).
Authors of publication	Li, Feng; Sevov, Slavi C.
Journal of publication	Inorganic chemistry
Year of publication	2015
Journal volume	54
Journal issue	16
Pages of publication	8121 - 8125
a	38.399 ± 0.003 Å
b	27.38 ± 0.003 Å
c	30.128 ± 0.002 Å
α	90°
β	91.359 ± 0.002°
γ	90°
Cell volume	31667 ± 5 Å³
Cell temperature	120 ± 2 K
Ambient diffraction temperature	120 ± 2 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0647
Residual factor for significantly intense reflections	0.044
Weighted residual factors for significantly intense reflections	0.0937
Weighted residual factors for all reflections included in the refinement	0.1054
Goodness-of-fit parameter for all reflections included in the refinement	1.118
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
160497 (current)	2015-10-06	cif/ Updating files of 4344046, 4344047 Original log message: Adding full bibliography for 4344046--4344047.cif.	4344047.cif
152939	2015-08-06	cif/ Adding structures of 4344047 via cif-deposit CGI script.	4344047.cif