Crystallography Open Database

Information card for entry 4344048

Preview

Coordinates	4344048.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	Ge6 H34 K6 O38
Calculated formula	Ge6 H34 K6 O38
Title of publication	Potassium, Cesium, and Ammonium Peroxogermanates with Inorganic Hexanuclear Peroxo Bridged Germanium Anion Isolated from Aqueous Solution.
Authors of publication	Medvedev, Alexander G.; Mikhaylov, Alexey A.; Churakov, Andrei V.; Vener, Mikhail V.; Tripol'skaya, Tatiana A.; Cohen, Shmuel; Lev, Ovadia; Prikhodchenko, Petr V.
Journal of publication	Inorganic chemistry
Year of publication	2015
Journal volume	54
Journal issue	16
Pages of publication	8058 - 8065
a	9.9695 ± 0.0013 Å
b	12.7455 ± 0.0016 Å
c	14.6041 ± 0.0019 Å
α	90°
β	107.188 ± 0.002°
γ	90°
Cell volume	1772.8 ± 0.4 Å³
Cell temperature	110 ± 2 K
Ambient diffraction temperature	110 ± 2 K
Number of distinct elements	4
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0181
Residual factor for significantly intense reflections	0.0169
Weighted residual factors for significantly intense reflections	0.0421
Weighted residual factors for all reflections included in the refinement	0.0426
Goodness-of-fit parameter for all reflections included in the refinement	1.068
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
160501 (current)	2015-10-06	cif/ Updating files of 4344048, 4344049 Original log message: Adding full bibliography for 4344048--4344049.cif.	4344048.cif
152940	2015-08-06	cif/ Adding structures of 4344048 via cif-deposit CGI script.	4344048.cif