Crystallography Open Database

Information card for entry 4344049

Preview

Coordinates	4344049.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	Cs4.2 Ge6 H29.2 N1.8 O32
Calculated formula	Cs4.2012 Ge6 H29.1952 N1.7988 O32
Title of publication	Potassium, Cesium, and Ammonium Peroxogermanates with Inorganic Hexanuclear Peroxo Bridged Germanium Anion Isolated from Aqueous Solution.
Authors of publication	Medvedev, Alexander G.; Mikhaylov, Alexey A.; Churakov, Andrei V.; Vener, Mikhail V.; Tripol'skaya, Tatiana A.; Cohen, Shmuel; Lev, Ovadia; Prikhodchenko, Petr V.
Journal of publication	Inorganic chemistry
Year of publication	2015
Journal volume	54
Journal issue	16
Pages of publication	8058 - 8065
a	7.896 ± 0.0008 Å
b	10.2383 ± 0.0011 Å
c	10.4517 ± 0.0011 Å
α	90.296 ± 0.001°
β	97.123 ± 0.001°
γ	90.829 ± 0.001°
Cell volume	838.3 ± 0.15 Å³
Cell temperature	183 ± 2 K
Ambient diffraction temperature	183 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0202
Residual factor for significantly intense reflections	0.0189
Weighted residual factors for significantly intense reflections	0.0459
Weighted residual factors for all reflections included in the refinement	0.0464
Goodness-of-fit parameter for all reflections included in the refinement	1.151
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
176429 (current)	2016-02-13	cif/ (antanas@kurmis) Replacing _cod_chemical_formula_sum_orig tag with _cod_original_formula_sum tag in multiple entries since the replaced tag is deprecated according to the COD CIF dictionary.	4344049.cif
160501	2015-10-06	cif/ Updating files of 4344048, 4344049 Original log message: Adding full bibliography for 4344048--4344049.cif.	4344049.cif
152941	2015-08-06	cif/ Adding structures of 4344049 via cif-deposit CGI script.	4344049.cif