Crystallography Open Database

Information card for entry 4347921

Preview

Coordinates	4347921.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C27 H39 F3 I N3 Si3 U
Calculated formula	C27 H39 F3 I N3 Si3 U
SMILES	[U]1(I)(N([Si](C)(C)C)c2c(cccc2)F)(N([Si](C)(C)C)c2c(cccc2)[F]1)N([Si](C)(C)C)c1c(cccc1)F
Title of publication	Cerium(III) and Uranium(IV) Complexes of the 2-Fluorophenyl Trimethylsilyl Amide Ligand: C-F →Ln/An Interactions that Modulate the Coordination Spheres of f-Block Elements.
Authors of publication	Yin, Haolin; Carroll, Patrick J.; Schelter, Eric J.
Journal of publication	Inorganic chemistry
Year of publication	2016
Journal volume	55
Journal issue	11
Pages of publication	5684 - 5692
a	10.4057 ± 0.0009 Å
b	11.0327 ± 0.0008 Å
c	16.1084 ± 0.0013 Å
α	85.395 ± 0.003°
β	79.603 ± 0.003°
γ	68.152 ± 0.002°
Cell volume	1688.1 ± 0.2 Å³
Cell temperature	100 K
Ambient diffraction temperature	100 ± 1 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0157
Residual factor for significantly intense reflections	0.0146
Weighted residual factors for significantly intense reflections	0.0354
Weighted residual factors for all reflections included in the refinement	0.0364
Goodness-of-fit parameter for all reflections included in the refinement	1.067
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
232587 (current)	2019-11-23	cif/ Adding structures of 4347917, 4347918, 4347919, 4347920, 4347921, 4347922 via cif-deposit CGI script.	4347921.cif