Crystallography Open Database

Information card for entry 4348013

Preview

Coordinates	4348013.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C27.5 H70 Cs2 N6 Si4
Calculated formula	C27.5 H70 Cs2 N6 Si4
Title of publication	Structural Studies of Cesium, Lithium/Cesium, and Sodium/Cesium Bis(trimethylsilyl)amide (HMDS) Complexes.
Authors of publication	Ojeda-Amador, Ana I; Martínez-Martínez, Antonio J; Kennedy, Alan R.; O'Hara, Charles T
Journal of publication	Inorganic chemistry
Year of publication	2016
Journal volume	55
Journal issue	11
Pages of publication	5719 - 5728
a	11.0696 ± 0.0005 Å
b	13.2566 ± 0.0007 Å
c	16.0829 ± 0.0007 Å
α	106.321 ± 0.004°
β	98.475 ± 0.004°
γ	95.449 ± 0.004°
Cell volume	2217.01 ± 0.19 Å³
Cell temperature	123 ± 2 K
Ambient diffraction temperature	123 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0407
Residual factor for significantly intense reflections	0.0286
Weighted residual factors for significantly intense reflections	0.0638
Weighted residual factors for all reflections included in the refinement	0.0725
Goodness-of-fit parameter for all reflections included in the refinement	1.102
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
232638 (current)	2019-11-23	cif/ Adding structures of 4348008, 4348009, 4348010, 4348011, 4348012, 4348013, 4348014 via cif-deposit CGI script.	4348013.cif