Crystallography Open Database

Information card for entry 4348843

Preview

Coordinates	4348843.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C23 H40 I2 N2 Si2
Calculated formula	C23 H40 I2 N2 Si2
SMILES	C1(C(CC(C)(C)N1c1c(C(C)C)cccc1C(C)C)(C)C)=[Si](I)(I)=N[Si](C)(C)C
Title of publication	Synthesis of a Bent 2-Silaallene with a Perturbed Electronic Structure from a Cyclic Alkyl(amino) Carbene-Diiodosilylene.
Authors of publication	Li, Yan; Chan, Yuk-Chi; Li, Yongxin; Purushothaman, Indu; De, Susmita; Parameswaran, Pattiyil; So, Cheuk-Wai
Journal of publication	Inorganic chemistry
Year of publication	2016
Journal volume	55
Journal issue	17
Pages of publication	9091 - 9098
a	10.0645 ± 0.0019 Å
b	17.697 ± 0.003 Å
c	15.512 ± 0.003 Å
α	90°
β	90.888 ± 0.004°
γ	90°
Cell volume	2762.5 ± 0.9 Å³
Cell temperature	103 ± 2 K
Ambient diffraction temperature	103 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0992
Residual factor for significantly intense reflections	0.0599
Weighted residual factors for significantly intense reflections	0.14
Weighted residual factors for all reflections included in the refinement	0.1746
Goodness-of-fit parameter for all reflections included in the refinement	0.996
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
233423 (current)	2019-11-23	cif/ Adding structures of 4348842, 4348843, 4348844, 4348845, 4348846 via cif-deposit CGI script.	4348843.cif