Crystallography Open Database

Information card for entry 4348844

Preview

Coordinates	4348844.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C34.5 H55 I2 N3 Si
Calculated formula	C34.5 H55 I2 N3 Si
Title of publication	Synthesis of a Bent 2-Silaallene with a Perturbed Electronic Structure from a Cyclic Alkyl(amino) Carbene-Diiodosilylene.
Authors of publication	Li, Yan; Chan, Yuk-Chi; Li, Yongxin; Purushothaman, Indu; De, Susmita; Parameswaran, Pattiyil; So, Cheuk-Wai
Journal of publication	Inorganic chemistry
Year of publication	2016
Journal volume	55
Journal issue	17
Pages of publication	9091 - 9098
a	9.9332 ± 0.0009 Å
b	12.471 ± 0.0011 Å
c	16.4044 ± 0.0014 Å
α	109.388 ± 0.002°
β	97.093 ± 0.002°
γ	104.146 ± 0.003°
Cell volume	1811.7 ± 0.3 Å³
Cell temperature	103 ± 2 K
Ambient diffraction temperature	103 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1424
Residual factor for significantly intense reflections	0.0591
Weighted residual factors for significantly intense reflections	0.0858
Weighted residual factors for all reflections included in the refinement	0.1083
Goodness-of-fit parameter for all reflections included in the refinement	0.991
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
233423 (current)	2019-11-23	cif/ Adding structures of 4348842, 4348843, 4348844, 4348845, 4348846 via cif-deposit CGI script.	4348844.cif