Crystallography Open Database

Information card for entry 7002658

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Coordinates	7002658.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C64 H186 Cd Ge18 Si24
Calculated formula	C64 H186 Cd Ge18 Si24
Title of publication	[Si(SiMe3)3]6Ge18M (M = Zn, Cd, Hg): neutral metalloid cluster compounds of germanium as highly soluble building blocks for supramolecular chemistry
Authors of publication	Henke, Florian; Schenk, Christian; Schnepf, Andreas
Journal of publication	Dalton Transactions
Year of publication	2009
Journal issue	42
Pages of publication	9141
a	14.956 ± 0.003 Å
b	19.083 ± 0.004 Å
c	23.622 ± 0.005 Å
α	90°
β	92.23 ± 0.03°
γ	90°
Cell volume	6737 ± 2 Å³
Cell temperature	149 ± 2 K
Ambient diffraction temperature	149 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0574
Residual factor for significantly intense reflections	0.0397
Weighted residual factors for significantly intense reflections	0.0783
Weighted residual factors for all reflections included in the refinement	0.0835
Goodness-of-fit parameter for all reflections included in the refinement	1.04
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179730 (current)	2016-03-25	cif/7/00/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/00/26.	7002658.cif
120443	2014-07-15	Adding 17924 DOIs guessed from source file names.	7002658.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7002658.cif
1143	2010-05-03	cif/7/ Adding CIFs from Dalton-Trans-2009/ deposition.	7002658.cif