Crystallography Open Database

Information card for entry 7002659

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Coordinates	7002659.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C54 H162 Ge18 Si24 Zn
Calculated formula	C54 H162 Ge18 Si24.006 Zn
Title of publication	[Si(SiMe3)3]6Ge18M (M = Zn, Cd, Hg): neutral metalloid cluster compounds of germanium as highly soluble building blocks for supramolecular chemistry
Authors of publication	Henke, Florian; Schenk, Christian; Schnepf, Andreas
Journal of publication	Dalton Transactions
Year of publication	2009
Journal issue	42
Pages of publication	9141
a	17.325 ± 0.004 Å
b	25.671 ± 0.005 Å
c	15.773 ± 0.003 Å
α	90°
β	113.51 ± 0.03°
γ	90°
Cell volume	6433 ± 3 Å³
Cell temperature	149 ± 2 K
Ambient diffraction temperature	149 ± 2 K
Number of distinct elements	5
Space group number	12
Hermann-Mauguin space group symbol	C 1 2/m 1
Hall space group symbol	-C 2y
Residual factor for all reflections	0.0541
Residual factor for significantly intense reflections	0.0403
Weighted residual factors for significantly intense reflections	0.0941
Weighted residual factors for all reflections included in the refinement	0.0998
Goodness-of-fit parameter for all reflections included in the refinement	1.048
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179730 (current)	2016-03-25	cif/7/00/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/00/26.	7002659.cif
120443	2014-07-15	Adding 17924 DOIs guessed from source file names.	7002659.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7002659.cif
1143	2010-05-03	cif/7/ Adding CIFs from Dalton-Trans-2009/ deposition.	7002659.cif