Crystallography Open Database

Information card for entry 7004979

Preview

Coordinates	7004979.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C42 H62 Li2 N4 O2 Si2
Calculated formula	C42 H62 Li2 N4 O2 Si2
Title of publication	Synthesis and structures of selected benzamidinates of Li, Na, Al, Zr and Sn(II) using the C1-symmetric ligands [N(SiMe3)C(C6H4Me-4 or Ph)NPh]-.
Authors of publication	Hitchcock, Peter B.; Lappert, Michael F.; Merle, Philippe G.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2007
Journal issue	5
Pages of publication	585 - 594
a	9.861 ± 0.007 Å
b	9.412 ± 0.004 Å
c	23.889 ± 0.01 Å
α	90°
β	94.97 ± 0.06°
γ	90°
Cell volume	2209 ± 2 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.1046
Residual factor for significantly intense reflections	0.0736
Weighted residual factors for significantly intense reflections	0.199
Weighted residual factors for all reflections included in the refinement	0.2272
Goodness-of-fit parameter for all reflections included in the refinement	1.027
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179753 (current)	2016-03-25	cif/7/00/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/00/49.	7004979.cif
120443	2014-07-15	Adding 17924 DOIs guessed from source file names.	7004979.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7004979.cif
1186	2010-06-03	Adding CIFs from Chem-Comm-2010_20-22/ and Dalton-Trans-2007/ processing.	7004979.cif