Crystallography Open Database

Information card for entry 7004980

Preview

Coordinates	7004980.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	[MeAl{Me3SiNC(C6H4Me)NPh}2]
Formula	C35 H45 Al N4 Si2
Calculated formula	C35 H45 Al N4 Si2
Title of publication	Synthesis and structures of selected benzamidinates of Li, Na, Al, Zr and Sn(II) using the C1-symmetric ligands [N(SiMe3)C(C6H4Me-4 or Ph)NPh]-.
Authors of publication	Hitchcock, Peter B.; Lappert, Michael F.; Merle, Philippe G.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2007
Journal issue	5
Pages of publication	585 - 594
a	11.6469 ± 0.0004 Å
b	14.5539 ± 0.0003 Å
c	20.9017 ± 0.0006 Å
α	90°
β	90.016 ± 0.001°
γ	90°
Cell volume	3543 ± 0.17 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0865
Residual factor for significantly intense reflections	0.0519
Weighted residual factors for significantly intense reflections	0.1165
Weighted residual factors for all reflections included in the refinement	0.1334
Goodness-of-fit parameter for all reflections included in the refinement	1.014
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179753 (current)	2016-03-25	cif/7/00/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/00/49.	7004980.cif
120443	2014-07-15	Adding 17924 DOIs guessed from source file names.	7004980.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7004980.cif
1186	2010-06-03	Adding CIFs from Chem-Comm-2010_20-22/ and Dalton-Trans-2007/ processing.	7004980.cif