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Information card for entry 7004981
Preview
| Coordinates | 7004981.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Common name | [Al{Me3SiNC(PhMe)NPh}2(Cl/Me)] |
|---|---|
| Formula | C34.52 H43.56 Al Cl0.48 N4 Si2 |
| Calculated formula | C34.521 H42 Al Cl0.479 N4 Si2 |
| Title of publication | Synthesis and structures of selected benzamidinates of Li, Na, Al, Zr and Sn(II) using the C1-symmetric ligands [N(SiMe3)C(C6H4Me-4 or Ph)NPh]-. |
| Authors of publication | Hitchcock, Peter B.; Lappert, Michael F.; Merle, Philippe G. |
| Journal of publication | Dalton transactions (Cambridge, England : 2003) |
| Year of publication | 2007 |
| Journal issue | 5 |
| Pages of publication | 585 - 594 |
| a | 10.2505 ± 0.0003 Å |
| b | 12.4069 ± 0.0003 Å |
| c | 14.8217 ± 0.0003 Å |
| α | 105.102 ± 0.001° |
| β | 101.05 ± 0.001° |
| γ | 93.509 ± 0.001° |
| Cell volume | 1773.81 ± 0.08 Å3 |
| Cell temperature | 173 ± 2 K |
| Ambient diffraction temperature | 173 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0556 |
| Residual factor for significantly intense reflections | 0.0428 |
| Weighted residual factors for significantly intense reflections | 0.1088 |
| Weighted residual factors for all reflections included in the refinement | 0.117 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.016 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 179753 (current) | 2016-03-25 | cif/7/00/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/00/49. |
7004981.cif |
| 120443 | 2014-07-15 | Adding 17924 DOIs guessed from source file names. | 7004981.cif |
| 35909 | 2012-02-26 | cif/7/: reorganising range 7 into a prefix-directory tree. | 7004981.cif |
| 1186 | 2010-06-03 | Adding CIFs from Chem-Comm-2010_20-22/ and Dalton-Trans-2007/ processing. | 7004981.cif |
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Users of the data should acknowledge the original authors of the
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