Crystallography Open Database

Information card for entry 7008802

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Coordinates	7008802.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C29 H79 Ce Li2 O9 Si8
Calculated formula	C29 H79 Ce Li2 O9 Si8
Title of publication	The coordination chemistry of the C1-symmetric bis(silyl)methyl ligand [CH(SiMe3){SiMe(OMe)2}]- revisited: Li/M- (M = Zn, Tl, Ce), Li4- or Ce2-methoxy-bridged alkyls.
Authors of publication	Hitchcock, Peter B.; Huang, Qigu; Lappert, Michael F.; Zhou, Meisu
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2005
Journal issue	18
Pages of publication	2988 - 2993
a	9.6796 ± 0.0002 Å
b	12.6308 ± 0.0003 Å
c	22.7947 ± 0.0005 Å
α	74.111 ± 0.001°
β	80.214 ± 0.001°
γ	72.502 ± 0.001°
Cell volume	2544.7 ± 0.1 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0691
Residual factor for significantly intense reflections	0.0476
Weighted residual factors for significantly intense reflections	0.1038
Weighted residual factors for all reflections included in the refinement	0.1136
Goodness-of-fit parameter for all reflections included in the refinement	1.021
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179792 (current)	2016-03-25	cif/7/00/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/00/88.	7008802.cif
120443	2014-07-15	Adding 17924 DOIs guessed from source file names.	7008802.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7008802.cif
1504	2010-09-08	cif/7/ Adding data extracted from RSC 2005 and 2006 year publications.	7008802.cif