Crystallography Open Database

Information card for entry 7009154

Preview

Coordinates	7009154.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	Tri(tert.butyl)gallium-triethylantimon-adduct
Formula	C18 H42 Ga Sb
Calculated formula	C18 H42 Ga Sb
SMILES	[Ga]([Sb](CC)(CC)CC)(C(C)(C)C)(C(C)(C)C)C(C)(C)C
Title of publication	Synthesis and structural characterization of the first completely alkyl-substituted Ga‒Sb Lewis acid‒base adducts †
Authors of publication	Schulz, Stephan; Nieger, Martin
Journal of publication	Journal of the Chemical Society, Dalton Transactions
Year of publication	2000
Journal issue	5
Pages of publication	639
a	14.1615 ± 0.0003 Å
b	9.5735 ± 0.0002 Å
c	16.0291 ± 0.0004 Å
α	90°
β	90.905 ± 0.002°
γ	90°
Cell volume	2172.88 ± 0.08 Å³
Cell temperature	123 ± 2 K
Ambient diffraction temperature	123 ± 2 K
Number of distinct elements	4
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0435
Residual factor for significantly intense reflections	0.041
Weighted residual factors for significantly intense reflections	0.1127
Weighted residual factors for all reflections included in the refinement	0.114
Goodness-of-fit parameter for all reflections included in the refinement	1.148
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179795 (current)	2016-03-25	cif/7/00/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/00/91.	7009154.cif
120443	2014-07-15	Adding 17924 DOIs guessed from source file names.	7009154.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7009154.cif
3896	2010-12-08	cif/7/ Adding CIFs with data from Dalton-Trans-2004-2000/.	7009154.cif