Crystallography Open Database

Information card for entry 7009459

Preview

Coordinates	7009459.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C15 H34 As Cl2 P Pd
Calculated formula	C15 H34 As Cl2 P Pd
SMILES	[Pd]1([As](C[P]1(C(C)C)C(C)C)(C(C)(C)C)C(C)(C)C)(Cl)Cl
Title of publication	The first palladium(II) complexes containing arsino(phosphino)methanes as ligands †
Authors of publication	Schmidt, Ulrich; Ilg, Kerstin; Werner, Helmut
Journal of publication	Journal of the Chemical Society, Dalton Transactions
Year of publication	2000
Journal issue	7
Pages of publication	1005
a	18.408 ± 0.003 Å
b	8.1421 ± 0.0009 Å
c	14.335 ± 0.002 Å
α	90°
β	109.071 ± 0.018°
γ	90°
Cell volume	2030.6 ± 0.5 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0476
Residual factor for significantly intense reflections	0.0378
Weighted residual factors for significantly intense reflections	0.096
Weighted residual factors for all reflections included in the refinement	0.1001
Goodness-of-fit parameter for all reflections included in the refinement	1.01
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179798 (current)	2016-03-25	cif/7/00/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/00/94.	7009459.cif
120443	2014-07-15	Adding 17924 DOIs guessed from source file names.	7009459.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7009459.cif
11752	2011-02-18	cif/7/ Redepositing RSC CIFs that were formally processed with an old version of cif_fix_values script.	7009459.cif
3896	2010-12-08	cif/7/ Adding CIFs with data from Dalton-Trans-2004-2000/.	7009459.cif