Crystallography Open Database

Information card for entry 7009460

Preview

Coordinates	7009460.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C65 H88 As2 B Cl3 F24 P2 Pd2
Calculated formula	C65 H88 As2 B Cl3 F24 P2 Pd2
Title of publication	The first palladium(II) complexes containing arsino(phosphino)methanes as ligands †
Authors of publication	Schmidt, Ulrich; Ilg, Kerstin; Werner, Helmut
Journal of publication	Journal of the Chemical Society, Dalton Transactions
Year of publication	2000
Journal issue	7
Pages of publication	1005
a	14.487 ± 0.009 Å
b	17.323 ± 0.011 Å
c	17.554 ± 0.012 Å
α	112.46 ± 0.08°
β	96.69 ± 0.08°
γ	101.79 ± 0.08°
Cell volume	3892 ± 6 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	8
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0792
Residual factor for significantly intense reflections	0.0404
Weighted residual factors for significantly intense reflections	0.0827
Weighted residual factors for all reflections included in the refinement	0.0928
Goodness-of-fit parameter for all reflections included in the refinement	0.84
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179798 (current)	2016-03-25	cif/7/00/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/00/94.	7009460.cif
120443	2014-07-15	Adding 17924 DOIs guessed from source file names.	7009460.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7009460.cif
3896	2010-12-08	cif/7/ Adding CIFs with data from Dalton-Trans-2004-2000/.	7009460.cif