Crystallography Open Database

Information card for entry 7019445

7019444 << 7019445 >> 7019446

Preview

Coordinates	7019445.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C58 H74 N7 O2 Si2 Yb
Calculated formula	C58 H66 N7 O2 Si2 Yb
Title of publication	Synthesis, characterization of bridged bis(amidinate) lanthanide amides and their application as catalysts for addition of amines to nitriles for monosubstituted N-arylamidines.
Authors of publication	Li, Wenbo; Xue, Mingqiang; Xu, Fan; Tu, Jing; Zhang, Yong; Shen, Qi
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2012
Journal volume	41
Journal issue	27
Pages of publication	8252 - 8260
a	12.8432 ± 0.0009 Å
b	20.1542 ± 0.0013 Å
c	22.7598 ± 0.0015 Å
α	90°
β	97.886 ± 0.002°
γ	90°
Cell volume	5835.5 ± 0.7 Å³
Cell temperature	223 ± 2 K
Ambient diffraction temperature	223 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0971
Residual factor for significantly intense reflections	0.0742
Weighted residual factors for significantly intense reflections	0.1404
Weighted residual factors for all reflections included in the refinement	0.1505
Goodness-of-fit parameter for all reflections included in the refinement	1.187
Diffraction radiation wavelength	0.71075 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179898 (current)	2016-03-25	cif/7/01/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/01/94.	7019445.cif
120112	2014-07-12	Adding DOIs to range 7 structures.	7019445.cif
62869	2012-07-09	cif/ Adding structures of 7019440, 7019441, 7019442, 7019443, 7019444, 7019445, 7019446, 7019447 via cif-deposit CGI script.	7019445.cif