Crystallography Open Database

Information card for entry 7019446

7019445 << 7019446 >> 7019447

Preview

Coordinates	7019446.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C74 H100 N10 O2 Si4 Yb2
Calculated formula	C74 H84 N10 O2 Si4 Yb2
Title of publication	Synthesis, characterization of bridged bis(amidinate) lanthanide amides and their application as catalysts for addition of amines to nitriles for monosubstituted N-arylamidines.
Authors of publication	Li, Wenbo; Xue, Mingqiang; Xu, Fan; Tu, Jing; Zhang, Yong; Shen, Qi
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2012
Journal volume	41
Journal issue	27
Pages of publication	8252 - 8260
a	12.1228 ± 0.0006 Å
b	12.7576 ± 0.0007 Å
c	13.5956 ± 0.0006 Å
α	80.15 ± 0.005°
β	68.709 ± 0.004°
γ	84.206 ± 0.005°
Cell volume	1928.55 ± 0.18 Å³
Cell temperature	223 ± 2 K
Ambient diffraction temperature	223 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0639
Residual factor for significantly intense reflections	0.052
Weighted residual factors for significantly intense reflections	0.097
Weighted residual factors for all reflections included in the refinement	0.1027
Goodness-of-fit parameter for all reflections included in the refinement	1.125
Diffraction radiation wavelength	0.71075 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179898 (current)	2016-03-25	cif/7/01/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/01/94.	7019446.cif
120112	2014-07-12	Adding DOIs to range 7 structures.	7019446.cif
62869	2012-07-09	cif/ Adding structures of 7019440, 7019441, 7019442, 7019443, 7019444, 7019445, 7019446, 7019447 via cif-deposit CGI script.	7019446.cif