Crystallography Open Database

Information card for entry 7021007

Preview

Coordinates	7021007.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C70.85 H156.4 Cl4 Cu4 Ge6 N12 Si6
Calculated formula	C70.85 H156.4 Cl4 Cu4 Ge6 N12 Si6
Title of publication	Heavier carbene analogues and their derivatives as κ-El, κ(2)-El,N, and κ(2)-N,N' ligands: different reactivity patterns for acyclic and cyclic diamidogermylenes and -stannylenes.
Authors of publication	West, Joseph K.; Fondong, Gregory L.; Noll, Bruce C.; Stahl, Lothar
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2013
Journal volume	42
Journal issue	11
Pages of publication	3835 - 3842
a	12.6839 ± 0.0014 Å
b	15.6668 ± 0.0017 Å
c	16.3267 ± 0.0017 Å
α	101.88 ± 0.0017°
β	111.442 ± 0.0016°
γ	108.31 ± 0.0016°
Cell volume	2671.5 ± 0.5 Å³
Cell temperature	173.15 K
Ambient diffraction temperature	173.15 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0454
Residual factor for significantly intense reflections	0.0371
Weighted residual factors for significantly intense reflections	0.106
Weighted residual factors for all reflections included in the refinement	0.1122
Goodness-of-fit parameter for all reflections included in the refinement	1.044
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
176453 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 7.	7021007.cif
75551	2013-03-10	cif/ Adding structures of 7021007, 7021008, 7021009 via cif-deposit CGI script.	7021007.cif