Crystallography Open Database

Information card for entry 7024698

Preview

Coordinates	7024698.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C71 H71 La N O3 S Si4
Calculated formula	C71 H71 La N O3 S Si4
Title of publication	Group 3 metal complexes supported by tridentate pyridine- and thiophene-linked bis(naphtholate) ligands: synthesis, structure, and use in stereoselective ring-opening polymerization of racemic lactide and beta-butyrolactone.
Authors of publication	Grunova, Ekaterina; Kirillov, Evgueni; Roisnel, Thierry; Carpentier, Jean-François
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2010
Journal volume	39
Journal issue	29
Pages of publication	6739 - 6752
a	38.9355 ± 0.0014 Å
b	15.5687 ± 0.0006 Å
c	22.9647 ± 0.0008 Å
α	90°
β	113.803 ± 0.002°
γ	90°
Cell volume	12736.5 ± 0.8 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	7
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0693
Residual factor for significantly intense reflections	0.0426
Weighted residual factors for significantly intense reflections	0.09
Weighted residual factors for all reflections included in the refinement	0.1018
Goodness-of-fit parameter for all reflections included in the refinement	1.02
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179951 (current)	2016-03-25	cif/7/02/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/02/46.	7024698.cif
92639	2014-01-12	cif/ Adding structures of 7024694, 7024695, 7024696, 7024697, 7024698, 7024699 via cif-deposit CGI script.	7024698.cif