Crystallography Open Database

Information card for entry 7027377

Preview

Coordinates	7027377.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C28 H39 Cl F6 P2 Ru Te4
Calculated formula	C28 H39 Cl F6 P2 Ru Te4
Title of publication	Platinum metal ditelluroether complexes: synthesis, spectroscopic and structural studies of [M(L‒L)2][PF6]2 [M = Pd or Pt, L‒L = RTe(CH2)3TeR (R = Me or Ph) or C6H4(TeMe)2-o], [Rh(L‒L)2Cl2]PF6, [Ru(L‒L)2X2] (X = Cl, Br or I) and [Ru(L‒L)2(PPh3)Cl]PF6
Authors of publication	Levason, William; Orchard, Simon D.; Reid, Gillian; Tolhurst, Vicki-Ann
Journal of publication	Journal of the Chemical Society, Dalton Transactions
Year of publication	1999
Journal issue	12
Pages of publication	2071
a	9.296 ± 0.003 Å
b	30.811 ± 0.002 Å
c	12.732 ± 0.003 Å
α	90°
β	105.4 ± 0.02°
γ	90°
Cell volume	3515.8 ± 1.5 Å³
Cell temperature	150 K
Ambient diffraction temperature	150 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for significantly intense reflections	0.0448
Weighted residual factors for significantly intense reflections	0.0508
Goodness-of-fit parameter for significantly intense reflections	1.63
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKalpha
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176453 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 7.	7027377.cif
130086	2015-01-23	cod/ (robertas@burundukas) The 'cif_fix_values' program was applied to CIFs that have generated the validation messages containing tag '_exptl_crystal_density_meas'. 16946 CIFs had a values that were perceived as 'not measured' and they were changed to '?'. The total of 17089 CIFs was changed. Those that were not corrected by 'cif_fix_values' were reformatted by the parser (e.g. a doi tag was moved to another place). The processing command was: mysql -u cod_reader -h www.crystallography.net cod -e \ 'select distinct codid from validation \ where message like \ "%tag%_exptl_crystal_density_meas'\''%"' -NB \ \| xargs -i sh -c 'cif_fix_values {} \ \| cif_filter --add-cif-header {} \ \| sponge {}'	7027377.cif
95325	2014-01-28	cif/ Adding structures of 7027376, 7027377, 7027378 via cif-deposit CGI script.	7027377.cif