Crystallography Open Database

Information card for entry 7027378

Preview

Coordinates	7027378.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C18 H23 F12 N P2 Pd Te4
Calculated formula	C18 H20 F12 N2 P2 Pd Te4
Title of publication	Platinum metal ditelluroether complexes: synthesis, spectroscopic and structural studies of [M(L‒L)2][PF6]2 [M = Pd or Pt, L‒L = RTe(CH2)3TeR (R = Me or Ph) or C6H4(TeMe)2-o], [Rh(L‒L)2Cl2]PF6, [Ru(L‒L)2X2] (X = Cl, Br or I) and [Ru(L‒L)2(PPh3)Cl]PF6
Authors of publication	Levason, William; Orchard, Simon D.; Reid, Gillian; Tolhurst, Vicki-Ann
Journal of publication	Journal of the Chemical Society, Dalton Transactions
Year of publication	1999
Journal issue	12
Pages of publication	2071
a	8.9645 ± 0.0006 Å
b	18.896 ± 0.002 Å
c	8.9325 ± 0.0005 Å
α	94.536 ± 0.006°
β	95.649 ± 0.005°
γ	99.533 ± 0.007°
Cell volume	1477.9 ± 0.2 Å³
Cell temperature	150 K
Ambient diffraction temperature	150 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for significantly intense reflections	0.0309
Weighted residual factors for significantly intense reflections	0.0362
Goodness-of-fit parameter for significantly intense reflections	1.933
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKalpha
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176453 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 7.	7027378.cif
95325	2014-01-28	cif/ Adding structures of 7027376, 7027377, 7027378 via cif-deposit CGI script.	7027378.cif