Crystallography Open Database

Information card for entry 7035228

Preview

Coordinates	7035228.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C10 H20 F6 O2 P2 Pb Si
Calculated formula	C10 H20 F6 O2 P2 Pb Si
Title of publication	Lead(ii) nitrate and hexafluorosilicate complexes with neutral diphosphine coordination.
Authors of publication	Burt, Jennifer; Grantham, William; Levason, William; Reid, Gillian
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2015
Journal volume	44
Journal issue	25
Pages of publication	11533 - 11541
a	6.6164 ± 0.0017 Å
b	10.637 ± 0.003 Å
c	12.354 ± 0.003 Å
α	93.58 ± 0.006°
β	93.952 ± 0.003°
γ	100.854 ± 0.006°
Cell volume	849.3 ± 0.4 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0276
Residual factor for significantly intense reflections	0.0261
Weighted residual factors for significantly intense reflections	0.0643
Weighted residual factors for all reflections included in the refinement	0.0646
Goodness-of-fit parameter for all reflections included in the refinement	0.996
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
143539 (current)	2015-07-11	cif/ Updating files of 7035226, 7035227, 7035228, 7035229, 7035230, 7035231 Original log message: Adding full bibliography for 7035226--7035231.cif.	7035228.cif
137180	2015-05-22	cif/ Adding structures of 7035226, 7035227, 7035228, 7035229, 7035230, 7035231 via cif-deposit CGI script.	7035228.cif