Crystallography Open Database

Information card for entry 7035229

Preview

Coordinates	7035229.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C19 H37 F6 N3 O3 P2 Pb Si
Calculated formula	C19 H37 F6 N3 O3 P2 Pb Si
SMILES	[Pb]1([P](c2ccccc2[P]1(C)C)(C)C)([F][Si](F)(F)(F)(F)F)[O]=CN(C)C.O=CN(C)C.O=CN(C)C
Title of publication	Lead(ii) nitrate and hexafluorosilicate complexes with neutral diphosphine coordination.
Authors of publication	Burt, Jennifer; Grantham, William; Levason, William; Reid, Gillian
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2015
Journal volume	44
Journal issue	25
Pages of publication	11533 - 11541
a	8.404 ± 0.002 Å
b	10.352 ± 0.003 Å
c	15.994 ± 0.005 Å
α	87.522 ± 0.007°
β	89.782 ± 0.006°
γ	86.063 ± 0.007°
Cell volume	1386.9 ± 0.7 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	8
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0477
Residual factor for significantly intense reflections	0.0425
Weighted residual factors for significantly intense reflections	0.0869
Weighted residual factors for all reflections included in the refinement	0.088
Goodness-of-fit parameter for all reflections included in the refinement	0.887
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
143539 (current)	2015-07-11	cif/ Updating files of 7035226, 7035227, 7035228, 7035229, 7035230, 7035231 Original log message: Adding full bibliography for 7035226--7035231.cif.	7035229.cif
137180	2015-05-22	cif/ Adding structures of 7035226, 7035227, 7035228, 7035229, 7035230, 7035231 via cif-deposit CGI script.	7035229.cif