Crystallography Open Database

Information card for entry 7035230

Preview

Coordinates	7035230.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C20 H48 N2 O10 P4 Pb
Calculated formula	C20 H48 N2 O10 P4 Pb
Title of publication	Lead(ii) nitrate and hexafluorosilicate complexes with neutral diphosphine coordination.
Authors of publication	Burt, Jennifer; Grantham, William; Levason, William; Reid, Gillian
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2015
Journal volume	44
Journal issue	25
Pages of publication	11533 - 11541
a	15.1483 ± 0.0005 Å
b	13.89 ± 0.0004 Å
c	16.2854 ± 0.0005 Å
α	90°
β	112.383 ± 0.003°
γ	90°
Cell volume	3168.45 ± 0.18 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0446
Residual factor for significantly intense reflections	0.031
Weighted residual factors for significantly intense reflections	0.0674
Weighted residual factors for all reflections included in the refinement	0.073
Goodness-of-fit parameter for all reflections included in the refinement	1.016
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
143539 (current)	2015-07-11	cif/ Updating files of 7035226, 7035227, 7035228, 7035229, 7035230, 7035231 Original log message: Adding full bibliography for 7035226--7035231.cif.	7035230.cif
137180	2015-05-22	cif/ Adding structures of 7035226, 7035227, 7035228, 7035229, 7035230, 7035231 via cif-deposit CGI script.	7035230.cif