Crystallography Open Database

Information card for entry 7035231

Preview

Coordinates	7035231.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C12.5 H33.5 B2 F8 N0.5 O3 P4 Pb
Calculated formula	C12.5 H32 B2 F8 N0.5 O3 P4 Pb
Title of publication	Lead(ii) nitrate and hexafluorosilicate complexes with neutral diphosphine coordination.
Authors of publication	Burt, Jennifer; Grantham, William; Levason, William; Reid, Gillian
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2015
Journal volume	44
Journal issue	25
Pages of publication	11533 - 11541
a	16.938 ± 0.006 Å
b	24.212 ± 0.009 Å
c	25.686 ± 0.01 Å
α	90°
β	90°
γ	90°
Cell volume	10534 ± 7 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	8
Space group number	70
Hermann-Mauguin space group symbol	F d d d
Hall space group symbol	-F 2uv 2vw
Residual factor for all reflections	0.0613
Residual factor for significantly intense reflections	0.0527
Weighted residual factors for significantly intense reflections	0.1033
Weighted residual factors for all reflections included in the refinement	0.1075
Goodness-of-fit parameter for all reflections included in the refinement	1.146
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
176429 (current)	2016-02-13	cif/ (antanas@kurmis) Replacing _cod_chemical_formula_sum_orig tag with _cod_original_formula_sum tag in multiple entries since the replaced tag is deprecated according to the COD CIF dictionary.	7035231.cif
143539	2015-07-11	cif/ Updating files of 7035226, 7035227, 7035228, 7035229, 7035230, 7035231 Original log message: Adding full bibliography for 7035226--7035231.cif.	7035231.cif
137180	2015-05-22	cif/ Adding structures of 7035226, 7035227, 7035228, 7035229, 7035230, 7035231 via cif-deposit CGI script.	7035231.cif