Crystallography Open Database

Information card for entry 7038481

Preview

Coordinates	7038481.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C31.5 H50 Bi Cl2 N Si
Calculated formula	C31.5 H50 Bi Cl2 N Si
Title of publication	Synthesis of mono-, di-, and triaminobismuthanes and observation of C-C coupling of aromatic systems with bismuth(iii) chloride.
Authors of publication	Hering-Junghans, Christian; Schulz, Axel; Thomas, Max; Villinger, Alexander
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2016
Journal volume	45
Journal issue	14
Pages of publication	6053 - 6059
a	10.177 ± 0.0005 Å
b	10.7624 ± 0.0005 Å
c	16.328 ± 0.0007 Å
α	93.75 ± 0.002°
β	101.264 ± 0.002°
γ	105.923 ± 0.002°
Cell volume	1673.17 ± 0.14 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0258
Residual factor for significantly intense reflections	0.0209
Weighted residual factors for significantly intense reflections	0.047
Weighted residual factors for all reflections included in the refinement	0.0485
Goodness-of-fit parameter for all reflections included in the refinement	1.038
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
181736 (current)	2016-04-05	cif/ Updating files of 7038481, 7038482, 7038483, 7038484, 7038485, 7038486, 7038487, 7038488, 7038489, 7038490, 7038491, 7038492, 7038493, 7038494, 7038495, 7038496, 7038497, 7038498, 7038499 Original log message: Adding full bibliography for 7038481--7038499.cif.	7038481.cif
176784	2016-02-20	cif/ Adding structures of 7038481, 7038482, 7038483, 7038484, 7038485, 7038486, 7038487, 7038488, 7038489, 7038490, 7038491, 7038492, 7038493, 7038494, 7038495, 7038496, 7038497, 7038498, 7038499 via cif-deposit CGI script.	7038481.cif