Crystallography Open Database

Information card for entry 7038482

Preview

Coordinates	7038482.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C42 H76 N2 Si2
Calculated formula	C42 H76 N2 Si2
Title of publication	Synthesis of mono-, di-, and triaminobismuthanes and observation of C-C coupling of aromatic systems with bismuth(iii) chloride.
Authors of publication	Hering-Junghans, Christian; Schulz, Axel; Thomas, Max; Villinger, Alexander
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2016
Journal volume	45
Journal issue	14
Pages of publication	6053 - 6059
a	10.3047 ± 0.0009 Å
b	28.762 ± 0.003 Å
c	14.6355 ± 0.0011 Å
α	90°
β	94.693 ± 0.004°
γ	90°
Cell volume	4323.2 ± 0.7 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	4
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.1196
Residual factor for significantly intense reflections	0.0549
Weighted residual factors for significantly intense reflections	0.118
Weighted residual factors for all reflections included in the refinement	0.1466
Goodness-of-fit parameter for all reflections included in the refinement	1.006
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
181736 (current)	2016-04-05	cif/ Updating files of 7038481, 7038482, 7038483, 7038484, 7038485, 7038486, 7038487, 7038488, 7038489, 7038490, 7038491, 7038492, 7038493, 7038494, 7038495, 7038496, 7038497, 7038498, 7038499 Original log message: Adding full bibliography for 7038481--7038499.cif.	7038482.cif
176784	2016-02-20	cif/ Adding structures of 7038481, 7038482, 7038483, 7038484, 7038485, 7038486, 7038487, 7038488, 7038489, 7038490, 7038491, 7038492, 7038493, 7038494, 7038495, 7038496, 7038497, 7038498, 7038499 via cif-deposit CGI script.	7038482.cif