Crystallography Open Database

Information card for entry 7049550

Preview

Coordinates	7049550.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C32 H44 Co2 Mo10 N8 O50 Zn2
Calculated formula	C32 H44 Co2 Mo10 N8 O50 Zn2
Title of publication	Syntheses, structures and catalytic properties of Evans-Showell-type polyoxometalate-based 3D metal-organic complexes constructed from the semi-rigid bis(pyridylformyl)piperazine ligand and transition metals.
Authors of publication	Li, Feng-Cai; Tan, Li-Kun; Li, Xi-Li; Kong, Hua-Jie; Ge, Li-Ming; Yue, Ling-Yu; Han, Li-Feng
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2019
Journal volume	48
Journal issue	17
Pages of publication	5831 - 5841
a	21.544 ± 0.002 Å
b	14.2328 ± 0.0012 Å
c	24.246 ± 0.003 Å
α	90°
β	104.817 ± 0.01°
γ	90°
Cell volume	7187.4 ± 1.3 Å³
Cell temperature	298.15 K
Ambient diffraction temperature	298.15 K
Number of distinct elements	7
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.1109
Residual factor for significantly intense reflections	0.0921
Weighted residual factors for significantly intense reflections	0.2025
Weighted residual factors for all reflections included in the refinement	0.2129
Goodness-of-fit parameter for all reflections included in the refinement	1.091
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
224117 (current)	2019-11-07	cif/ Updating files of 7049549, 7049550 Original log message: Adding full bibliography for 7049549--7049550.cif.	7049550.cif
214456	2019-04-03	cif/ Adding structures of 7049549, 7049550 via cif-deposit CGI script.	7049550.cif