Crystallography Open Database

Information card for entry 7051864

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Structure parameters

Formula	C95 H134 N6 O2 Pb2
Calculated formula	C95 H134 N6 O2 Pb2
Title of publication	Thermally stable lead(ii) amidinates and guanidinates
Authors of publication	Stasch, Andreas; Forsyth, Craig M.; Jones, Cameron; Junk, Peter C.
Journal of publication	New Journal of Chemistry
Year of publication	2008
Journal volume	32
Journal issue	5
Pages of publication	829
a	10.0458 ± 0.0002 Å
b	24.5646 ± 0.0006 Å
c	17.3771 ± 0.0004 Å
α	90°
β	97.058 ± 0.001°
γ	90°
Cell volume	4255.67 ± 0.17 Å³
Cell temperature	123 ± 2 K
Ambient diffraction temperature	123 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0915
Residual factor for significantly intense reflections	0.0547
Weighted residual factors for significantly intense reflections	0.0723
Weighted residual factors for all reflections included in the refinement	0.0796
Goodness-of-fit parameter for all reflections included in the refinement	1.047
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
301851 (current)	2025-08-21	Add cross-references to PubChem compounds in COD range 7/05/ Each referenced PubChem compound corresponds to the full crystal structure.	7051864.cif
180072	2016-03-26	cif/7/05/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/05/18.	7051864.cif
120112	2014-07-12	Adding DOIs to range 7 structures.	7051864.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7051864.cif
1173	2010-05-16	cif/7/: adding data from Dalton-Trans-2008, New-J-Chem-2008, Org-Biomol-Chem-2008 and RSC-2008 processing.	7051864.cif