Crystallography Open Database

Information card for entry 7051865

Preview

Coordinates	7051865.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C50 H70 N4 Pb
Calculated formula	C50 H70 N4 Pb
Title of publication	Thermally stable lead(ii) amidinates and guanidinates
Authors of publication	Stasch, Andreas; Forsyth, Craig M.; Jones, Cameron; Junk, Peter C.
Journal of publication	New Journal of Chemistry
Year of publication	2008
Journal volume	32
Journal issue	5
Pages of publication	829
a	14.9163 ± 0.0003 Å
b	16.1789 ± 0.0003 Å
c	20.8178 ± 0.0005 Å
α	90°
β	110.09 ± 0.001°
γ	90°
Cell volume	4718.26 ± 0.17 Å³
Cell temperature	123 ± 2 K
Ambient diffraction temperature	123 ± 2 K
Number of distinct elements	4
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0959
Residual factor for significantly intense reflections	0.0576
Weighted residual factors for significantly intense reflections	0.1298
Weighted residual factors for all reflections included in the refinement	0.1455
Goodness-of-fit parameter for all reflections included in the refinement	1.053
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
180072 (current)	2016-03-26	cif/7/05/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/05/18.	7051865.cif
120112	2014-07-12	Adding DOIs to range 7 structures.	7051865.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7051865.cif
1173	2010-05-16	cif/7/: adding data from Dalton-Trans-2008, New-J-Chem-2008, Org-Biomol-Chem-2008 and RSC-2008 processing.	7051865.cif